Synthesis of nanocrystalline lead oxide particles by ultrasonic spray pyrolysis method

Burcak Ebin, Sebahattin Gurmen*, Cuneyt Arslan

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Özet

Lead oxide is a very important metal oxide semiconductor and considerable progresses have been made in the study of the production and applications such as in storage battaries, gas sensors and pigments. Nanocrystalline lead oxide particles were synthesized by ultrasonic spray pyrolysis method (USP) using lead nitrate solution under air flow rate at 600°C. Characterization studies of the nanocrystalline particles conducted on not only size and shape morphology of the particles, but also chemical composition, phase determination, crystal size, and band gap energy of the particles by the help of scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and UV-vis spectrophotometer. Analyses show that spherical PbO particles are in submicron range, and otherwise their crystalline size was determined 38 nm using Scherrer formulation.

Orijinal dilİngilizce
Ana bilgisayar yayını başlığıProceedings of the World Powder Metallurgy Congress and Exhibition, World PM 2010
YayınlayanEuropean Powder Metallurgy Association (EPMA)
ISBN (Basılı)9781899072194
Yayın durumuYayınlandı - 2010
EtkinlikWorld Powder Metallurgy Congress and Exhibition, World PM 2010 - Florence, Italy
Süre: 10 Eki 201014 Eki 2010

Yayın serisi

AdıProceedings of the World Powder Metallurgy Congress and Exhibition, World PM 2010
Hacim1

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???event.eventtypes.event.conference???World Powder Metallurgy Congress and Exhibition, World PM 2010
Ülke/BölgeItaly
ŞehirFlorence
Periyot10/10/1014/10/10

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