Synthesis of Nanocrystalline Cu3B2O6 Particles by Ultrasonic Spray Pyrolysis Method

Burcak Ebin; Sebahattin Gurmen; Cuneyt Arslan

doi:10.1002/9781118062173.ch80

Synthesis of Nanocrystalline Cu₃B₂O₆ Particles by Ultrasonic Spray Pyrolysis Method

Burcak Ebin^*
, Sebahattin Gurmen
, Cuneyt Arslan

^*Bu çalışma için yazışmadan sorumlu yazar

Metalurji ve Malzeme Müh.Böl.

Istanbul Technical University

Araştırma çıktısı: Kitap/Rapor/Konferans Bildirisinde Bölüm › Bölüm › Hakem

Özet

Nanocrystalline CU₃B₂O₆ particles were produced by ultrasonic spray pyrolysis (USP) method using aqueous solution of copper nitrate and boric acid in desired concentration. Particles obtained thermal decomposition of precursor under constant air flow rate at 1000°C furnace temperature. Then samples were structurally characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS). The results show that nanocrystalline CU₃B₂O₆ particles in nearly spherical morphology were prepared successfully. Also, XRD analysis reveal that obtained CU₃B₂O₆ particles have anorthic crystal structure and their crystalline size are nearly 29 nm, which are calculated by Scherrer equation.

Orijinal dil	İngilizce
Ana bilgisayar yayını başlığı	Supplemental Proceedings
Ana bilgisayar yayını alt yazısı	General Paper Selections
Yayınlayan	John Wiley and Sons Inc.
Sayfalar	631-634
Sayfa sayısı	4
Hacim	3
ISBN (Elektronik)	9781118062173
ISBN (Basılı)	9781118029473
DOI'lar	https://doi.org/10.1002/9781118062173.ch80
Yayın durumu	Yayınlandı - 3 May 2011

Bibliyografik not

Publisher Copyright:
© 2011 The Minerals, Metals & Materials Society.

Belgeye Erişim

10.1002/9781118062173.ch80

Diğer Dosyalar ve Linkler

Link to publication in Scopus

Alıntı Yap

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title = "Synthesis of Nanocrystalline Cu3B2O6 Particles by Ultrasonic Spray Pyrolysis Method",

abstract = "Nanocrystalline CU3B2O6 particles were produced by ultrasonic spray pyrolysis (USP) method using aqueous solution of copper nitrate and boric acid in desired concentration. Particles obtained thermal decomposition of precursor under constant air flow rate at 1000°C furnace temperature. Then samples were structurally characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS). The results show that nanocrystalline CU3B2O6 particles in nearly spherical morphology were prepared successfully. Also, XRD analysis reveal that obtained CU3B2O6 particles have anorthic crystal structure and their crystalline size are nearly 29 nm, which are calculated by Scherrer equation.",

keywords = "Copper borate, Nanocrystalline, Ultrasonic spray pyrolysis",

author = "Burcak Ebin and Sebahattin Gurmen and Cuneyt Arslan",

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year = "2011",

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doi = "10.1002/9781118062173.ch80",

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AU - Gurmen, Sebahattin

AU - Arslan, Cuneyt

PY - 2011/5/3

Y1 - 2011/5/3

N2 - Nanocrystalline CU3B2O6 particles were produced by ultrasonic spray pyrolysis (USP) method using aqueous solution of copper nitrate and boric acid in desired concentration. Particles obtained thermal decomposition of precursor under constant air flow rate at 1000°C furnace temperature. Then samples were structurally characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS). The results show that nanocrystalline CU3B2O6 particles in nearly spherical morphology were prepared successfully. Also, XRD analysis reveal that obtained CU3B2O6 particles have anorthic crystal structure and their crystalline size are nearly 29 nm, which are calculated by Scherrer equation.

AB - Nanocrystalline CU3B2O6 particles were produced by ultrasonic spray pyrolysis (USP) method using aqueous solution of copper nitrate and boric acid in desired concentration. Particles obtained thermal decomposition of precursor under constant air flow rate at 1000°C furnace temperature. Then samples were structurally characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS). The results show that nanocrystalline CU3B2O6 particles in nearly spherical morphology were prepared successfully. Also, XRD analysis reveal that obtained CU3B2O6 particles have anorthic crystal structure and their crystalline size are nearly 29 nm, which are calculated by Scherrer equation.

KW - Copper borate

KW - Nanocrystalline

KW - Ultrasonic spray pyrolysis

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