Synthesis of Mn2O3 nanopowders with urea and citric acid by solution combustion route

Esma Yilmaz; M. Seref Sonmez; Bora Derin; Filiz Cinar Sahin; Onuralp Yucel

doi:10.1007/978-3-319-51493-2_5

Synthesis of Mn₂O₃ nanopowders with urea and citric acid by solution combustion route

Esma Yilmaz^*
, M. Seref Sonmez
, Bora Derin
, Filiz Cinar Sahin
, Onuralp Yucel

^*Bu çalışma için yazışmadan sorumlu yazar

Metalurji ve Malzeme Müh.Böl.

Istanbul Technical University

Araştırma sonucu: Kitap/Rapor/Konferans Bildirisinde Bölüm › Konferans katkısı › bilirkişi

3 Atıf (Scopus)

Özet

In this study, synthesis of Mn₂O₃ powders by solution combustion route was carried out. Urea (CH₄N₂O) and citric acid (C₆H₈O₇.H₂O) was used as a fuel material in solution combustion synthesis, while manganese nitrate (Mn(NO₃)₂.4H₂O) was used as an oxidant. Surface area of Mn₂O₃ synthesised by urea was calculated as 19,37 m²/g and 25,07 m²/g after the calcination at 400 °C and 500 °C, respectively. Surface area of Mn₂O₃ synthesised by citric acid was calculated as 63,77 m²/g when fuel/oxidizer was 1/1, ignition temperature of 250 °C and calcination temperature at 500 °C. Spherical particles of Mn₂O₃ having average particle size of 50–60 nm was synthesised by using urea, while foam like porous structure of Mn₂O₃ was obtained when citric acid was used as a fuel in solution combustion synthesis. Pore diameters between 27 and 55 nm was determined for this powders.

Orijinal dil	İngilizce
Ana bilgisayar yayını başlığı	TMS 2017 146th Annual Meeting
Yayınlayan	Springer International Publishing
Sayfalar	39-46
Sayfa sayısı	8
ISBN (Basılı)	9783319514925
DOI'lar	https://doi.org/10.1007/978-3-319-51493-2_5
Yayın durumu	Yayınlandı - 2017
Etkinlik	146th Annual Meeting and Exhibition Supplemental, TMS 2017 - San Diego, United States Süre: 26 Şub 2017 → 2 Mar 2017

Yayın serisi

Adı	Minerals, Metals and Materials Series
Hacim	Part F6
ISSN (Basılı)	2367-1181
ISSN (Elektronik)	2367-1696

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???event.eventtypes.event.conference???	146th Annual Meeting and Exhibition Supplemental, TMS 2017
Ülke/Bölge	United States
Şehir	San Diego
Periyot	26/02/17 → 2/03/17

Bibliyografik not

Publisher Copyright:
© The Minerals, Metals & Materials Society 2017.

Belgeye Erişim

10.1007/978-3-319-51493-2_5

Diğer Dosyalar ve Linkler

Link to publication in Scopus

Alıntı Yap

@inproceedings{5d230194c0c442d38327a803f0c787e0,

title = "Synthesis of Mn2O3 nanopowders with urea and citric acid by solution combustion route",

abstract = "In this study, synthesis of Mn2O3 powders by solution combustion route was carried out. Urea (CH4N2O) and citric acid (C6H8O7.H2O) was used as a fuel material in solution combustion synthesis, while manganese nitrate (Mn(NO3)2.4H2O) was used as an oxidant. Surface area of Mn2O3 synthesised by urea was calculated as 19,37 m2/g and 25,07 m2/g after the calcination at 400 °C and 500 °C, respectively. Surface area of Mn2O3 synthesised by citric acid was calculated as 63,77 m2/g when fuel/oxidizer was 1/1, ignition temperature of 250 °C and calcination temperature at 500 °C. Spherical particles of Mn2O3 having average particle size of 50–60 nm was synthesised by using urea, while foam like porous structure of Mn2O3 was obtained when citric acid was used as a fuel in solution combustion synthesis. Pore diameters between 27 and 55 nm was determined for this powders.",

keywords = "MnO, Nanopores, Nanopowders, Solution combustion synthesis",

author = "Esma Yilmaz and Sonmez, \{M. Seref\} and Bora Derin and Sahin, \{Filiz Cinar\} and Onuralp Yucel",

note = "Publisher Copyright: {\textcopyright} The Minerals, Metals \& Materials Society 2017.; 146th Annual Meeting and Exhibition Supplemental, TMS 2017 ; Conference date: 26-02-2017 Through 02-03-2017",

year = "2017",

doi = "10.1007/978-3-319-51493-2\_5",

language = "English",

isbn = "9783319514925",

series = "Minerals, Metals and Materials Series",

publisher = "Springer International Publishing",

pages = "39--46",

booktitle = "TMS 2017 146th Annual Meeting",

address = "Switzerland",

}

Yilmaz, E, Sonmez, MS , Derin, B , Sahin, FC & Yucel, O 2017, Synthesis of Mn₂O₃ nanopowders with urea and citric acid by solution combustion route. in TMS 2017 146th Annual Meeting. Minerals, Metals and Materials Series, hac. Part F6, Springer International Publishing, pp. 39-46, 146th Annual Meeting and Exhibition Supplemental, TMS 2017, San Diego, United States, 26/02/17. https://doi.org/10.1007/978-3-319-51493-2_5

Synthesis of Mn₂O₃ nanopowders with urea and citric acid by solution combustion route. / Yilmaz, Esma; Sonmez, M. Seref ; Derin, Bora et al.
TMS 2017 146th Annual Meeting. Springer International Publishing, 2017. p. 39-46 (Minerals, Metals and Materials Series; Hac. Part F6).

Araştırma sonucu: Kitap/Rapor/Konferans Bildirisinde Bölüm › Konferans katkısı › bilirkişi

TY - GEN

T1 - Synthesis of Mn2O3 nanopowders with urea and citric acid by solution combustion route

AU - Yilmaz, Esma

AU - Sonmez, M. Seref

AU - Derin, Bora

AU - Sahin, Filiz Cinar

AU - Yucel, Onuralp

PY - 2017

Y1 - 2017

N2 - In this study, synthesis of Mn2O3 powders by solution combustion route was carried out. Urea (CH4N2O) and citric acid (C6H8O7.H2O) was used as a fuel material in solution combustion synthesis, while manganese nitrate (Mn(NO3)2.4H2O) was used as an oxidant. Surface area of Mn2O3 synthesised by urea was calculated as 19,37 m2/g and 25,07 m2/g after the calcination at 400 °C and 500 °C, respectively. Surface area of Mn2O3 synthesised by citric acid was calculated as 63,77 m2/g when fuel/oxidizer was 1/1, ignition temperature of 250 °C and calcination temperature at 500 °C. Spherical particles of Mn2O3 having average particle size of 50–60 nm was synthesised by using urea, while foam like porous structure of Mn2O3 was obtained when citric acid was used as a fuel in solution combustion synthesis. Pore diameters between 27 and 55 nm was determined for this powders.

AB - In this study, synthesis of Mn2O3 powders by solution combustion route was carried out. Urea (CH4N2O) and citric acid (C6H8O7.H2O) was used as a fuel material in solution combustion synthesis, while manganese nitrate (Mn(NO3)2.4H2O) was used as an oxidant. Surface area of Mn2O3 synthesised by urea was calculated as 19,37 m2/g and 25,07 m2/g after the calcination at 400 °C and 500 °C, respectively. Surface area of Mn2O3 synthesised by citric acid was calculated as 63,77 m2/g when fuel/oxidizer was 1/1, ignition temperature of 250 °C and calcination temperature at 500 °C. Spherical particles of Mn2O3 having average particle size of 50–60 nm was synthesised by using urea, while foam like porous structure of Mn2O3 was obtained when citric acid was used as a fuel in solution combustion synthesis. Pore diameters between 27 and 55 nm was determined for this powders.

KW - MnO

KW - Nanopores

KW - Nanopowders

KW - Solution combustion synthesis

UR - https://www.scopus.com/pages/publications/85029781551

U2 - 10.1007/978-3-319-51493-2_5

DO - 10.1007/978-3-319-51493-2_5

M3 - Conference contribution

AN - SCOPUS:85029781551

SN - 9783319514925

T3 - Minerals, Metals and Materials Series

SP - 39

EP - 46

BT - TMS 2017 146th Annual Meeting

PB - Springer International Publishing

T2 - 146th Annual Meeting and Exhibition Supplemental, TMS 2017

Y2 - 26 February 2017 through 2 March 2017

ER -