Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

Kagan Benzesik; Filiz Çınar Şahin; Onuralp Yücel

doi:10.1007/978-3-031-80748-0_108

Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

Kagan Benzesik^*
, Filiz Çınar Şahin
, Onuralp Yücel

^*Bu çalışma için yazışmadan sorumlu yazar

Metalurji ve Malzeme Müh.Böl.

Araştırma çıktısı: Kitap/Rapor/Konferans Bildirisinde Bölüm › Konferans katkısı › Hakem

Özet

In this study, the SPS conditions of Li₄SiO₄ powders produced by combustion synthesis were investigated. There is no study on the sintering of Li₄SiO₄ powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.

Orijinal dil	İngilizce
Ana bilgisayar yayını başlığı	TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings
Yayınlayan	Springer Science and Business Media Deutschland GmbH
Sayfalar	1217-1226
Sayfa sayısı	10
ISBN (Basılı)	9783031807473
DOI'lar	https://doi.org/10.1007/978-3-031-80748-0_108
Yayın durumu	Yayınlandı - 2025
Etkinlik	154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025 - Las Vegas, United States Süre: 23 Mar 2025 → 27 Mar 2025

Yayın serisi

Adı	Minerals, Metals and Materials Series
ISSN (Basılı)	2367-1181
ISSN (Elektronik)	2367-1696

???event.eventtypes.event.conference???

???event.eventtypes.event.conference???	154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025
Ülke/Bölge	United States
Şehir	Las Vegas
Periyot	23/03/25 → 27/03/25

Bibliyografik not

Publisher Copyright:
© The Minerals, Metals & Materials Society 2025.

BM SKH

Bu sonuç, aşağıdaki Sürdürülebilir Kalkınma Hedefine/Hedeflerine katkıda bulunur

SKH 7 Erişilebilir ve Temiz Enerji

Belgeye Erişim

10.1007/978-3-031-80748-0_108

Diğer Dosyalar ve Linkler

Link to publication in Scopus

Alıntı Yap

@inproceedings{501c2e6d579143deb1fc5cb0499e9da4,

title = "Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders",

abstract = "In this study, the SPS conditions of Li4SiO4 powders produced by combustion synthesis were investigated. There is no study on the sintering of Li4SiO4 powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100\%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.",

keywords = "Compaction, Spark plasma sintering, Tritium breeding",

author = "Kagan Benzesik and {\c S}ahin, \{Filiz {\c C}ınar\} and Onuralp Y{\"u}cel",

note = "Publisher Copyright: {\textcopyright} The Minerals, Metals \& Materials Society 2025.; 154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025 ; Conference date: 23-03-2025 Through 27-03-2025",

year = "2025",

doi = "10.1007/978-3-031-80748-0\_108",

language = "English",

isbn = "9783031807473",

series = "Minerals, Metals and Materials Series",

publisher = "Springer Science and Business Media Deutschland GmbH",

pages = "1217--1226",

booktitle = "TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings",

address = "Germany",

}

Benzesik, K , Şahin, FÇ & Yücel, O 2025, Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders. in TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings. Minerals, Metals and Materials Series, Springer Science and Business Media Deutschland GmbH, pp. 1217-1226, 154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025, Las Vegas, United States, 23/03/25. https://doi.org/10.1007/978-3-031-80748-0_108

Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders. / Benzesik, Kagan ; Şahin, Filiz Çınar ; Yücel, Onuralp.
TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings. Springer Science and Business Media Deutschland GmbH, 2025. p. 1217-1226 (Minerals, Metals and Materials Series).

Araştırma çıktısı: Kitap/Rapor/Konferans Bildirisinde Bölüm › Konferans katkısı › Hakem

TY - GEN

T1 - Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

AU - Benzesik, Kagan

AU - Şahin, Filiz Çınar

AU - Yücel, Onuralp

PY - 2025

Y1 - 2025

N2 - In this study, the SPS conditions of Li4SiO4 powders produced by combustion synthesis were investigated. There is no study on the sintering of Li4SiO4 powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.

AB - In this study, the SPS conditions of Li4SiO4 powders produced by combustion synthesis were investigated. There is no study on the sintering of Li4SiO4 powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.

KW - Compaction

KW - Spark plasma sintering

KW - Tritium breeding

UR - https://www.scopus.com/pages/publications/105003993406

U2 - 10.1007/978-3-031-80748-0_108

DO - 10.1007/978-3-031-80748-0_108

M3 - Conference contribution

AN - SCOPUS:105003993406

SN - 9783031807473

T3 - Minerals, Metals and Materials Series

SP - 1217

EP - 1226

BT - TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings

PB - Springer Science and Business Media Deutschland GmbH

T2 - 154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025

Y2 - 23 March 2025 through 27 March 2025

ER -

Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

Özet

Yayın serisi

???event.eventtypes.event.conference???

Bibliyografik not

BM SKH

Belgeye Erişim

Diğer Dosyalar ve Linkler

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