Self-propagating High Temperature Synthesis of TiB2

Ahmet Turan; Mehmet Bugdayci; Onuralp Yucel

doi:10.1515/htmp-2014-0021

Self-propagating High Temperature Synthesis of TiB₂

Ahmet Turan^*
, Mehmet Bugdayci
, Onuralp Yucel

^*Bu çalışma için yazışmadan sorumlu yazar

Metalurji ve Malzeme Müh.Böl.

Istanbul Technical University

Araştırma sonucu: Dergiye katkı › Makale › bilirkişi

32 Atıf (Scopus)

Özet

Self-propagating high temperature synthesis (SHS) is a very important technique for the synthesis of high technology ceramics, metals and alloys. SHS parameters of TiB₂ were carried out in this study. Mg stoichiometry as reductant, process atmosphere and addition of NaCl and MgSO₄·7H₂O additives were investigated. HCl leaching was applied to SHS products to purify their TiB₂ contents. Stoichiometrically 100% Mg addition ratio and Ar atmosphere were determined as the optimum parameters. NaCl addition was also positively affected the specific surface area values. 11.78 m²/g specific surface area value was measured for 5.0% NaCl addition ratio.

Orijinal dil	İngilizce
Sayfa (başlangıç-bitiş)	185-193
Sayfa sayısı	9
Dergi	High Temperature Materials and Processes
Hacim	34
Basın numarası	2
DOI'lar	https://doi.org/10.1515/htmp-2014-0021
Yayın durumu	Yayınlandı - 1 Nis 2015

Bibliyografik not

Publisher Copyright:
© 2015 Walter De Gruyter. All rights reserved.

Belgeye Erişim

10.1515/htmp-2014-0021

Diğer Dosyalar ve Linkler

Link to publication in Scopus

Alıntı Yap

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abstract = "Self-propagating high temperature synthesis (SHS) is a very important technique for the synthesis of high technology ceramics, metals and alloys. SHS parameters of TiB2 were carried out in this study. Mg stoichiometry as reductant, process atmosphere and addition of NaCl and MgSO4·7H2O additives were investigated. HCl leaching was applied to SHS products to purify their TiB2 contents. Stoichiometrically 100\% Mg addition ratio and Ar atmosphere were determined as the optimum parameters. NaCl addition was also positively affected the specific surface area values. 11.78 m2/g specific surface area value was measured for 5.0\% NaCl addition ratio.",

keywords = "metallothermic reduction, self-propagating high temperature synthesis, titanium diboride",

author = "Ahmet Turan and Mehmet Bugdayci and Onuralp Yucel",

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AU - Turan, Ahmet

AU - Bugdayci, Mehmet

AU - Yucel, Onuralp

PY - 2015/4/1

Y1 - 2015/4/1

N2 - Self-propagating high temperature synthesis (SHS) is a very important technique for the synthesis of high technology ceramics, metals and alloys. SHS parameters of TiB2 were carried out in this study. Mg stoichiometry as reductant, process atmosphere and addition of NaCl and MgSO4·7H2O additives were investigated. HCl leaching was applied to SHS products to purify their TiB2 contents. Stoichiometrically 100% Mg addition ratio and Ar atmosphere were determined as the optimum parameters. NaCl addition was also positively affected the specific surface area values. 11.78 m2/g specific surface area value was measured for 5.0% NaCl addition ratio.

AB - Self-propagating high temperature synthesis (SHS) is a very important technique for the synthesis of high technology ceramics, metals and alloys. SHS parameters of TiB2 were carried out in this study. Mg stoichiometry as reductant, process atmosphere and addition of NaCl and MgSO4·7H2O additives were investigated. HCl leaching was applied to SHS products to purify their TiB2 contents. Stoichiometrically 100% Mg addition ratio and Ar atmosphere were determined as the optimum parameters. NaCl addition was also positively affected the specific surface area values. 11.78 m2/g specific surface area value was measured for 5.0% NaCl addition ratio.

KW - metallothermic reduction

KW - self-propagating high temperature synthesis

KW - titanium diboride

UR - https://www.scopus.com/pages/publications/84926368530

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DO - 10.1515/htmp-2014-0021

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VL - 34

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EP - 193

JO - High Temperature Materials and Processes

JF - High Temperature Materials and Processes

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