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Preparation and characterisation of WO3.1/3H2O thin films

Araştırma sonucu: Kitap/Rapor/Konferans Bildirisinde BölümKonferans katkısıbilirkişi

2 Atıf (Scopus)

Özet

The preparation and characterisation of WO3.1/3H2O phase, which is an intermediate to hexagonal tungsten oxide was performed. Tungsten oxide dihydrate was precipitated from acidified sodium tungstate solution. Two and three washing steps have been applied to the as-obtained amorphous gel. WO3.1/3H2O nanograins have been obtained after the hydrothermal process performed at 140°C, for 24 hours in an acid digestion bomb. A spin coater was used for thin film preparation. Structural, morphological and optical characterisation as well as electrochemical performance of thin films were determined by scanning electron microscopy, atomic force microscopy, Raman spectroscopy and cyclic voltammetry. The ion insertion properties of WO3.1/3H2O films show strong correlation to the close packed structure and to the presence of structural water.

Orijinal dilİngilizce
Ana bilgisayar yayını başlığıMaterials Science, Testing and Informatics III - Proceedings of the 5th Hungarian Conference on Materials Science, Testing and Informatics
YayınlayanTrans Tech Publications Ltd
Sayfalar113-120
Sayfa sayısı8
ISBN (Basılı)087849426X, 9780878494262
DOI'lar
Yayın durumuYayınlandı - 2007
Etkinlik5th Hungarian Conference on Materials Science, Testing and lnformatics - Balatonfured, Hungary
Süre: 9 Eki 200511 Eki 2005

Yayın serisi

AdıMaterials Science Forum
Hacim537-538
ISSN (Basılı)0255-5476
ISSN (Elektronik)1662-9752

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???event.eventtypes.event.conference???5th Hungarian Conference on Materials Science, Testing and lnformatics
Ülke/BölgeHungary
ŞehirBalatonfured
Periyot9/10/0511/10/05

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