Analysis of anthraquinones in Rumex crispus by micellar electrokinetic chromatography

Selda Başkan; Ayşe Daut-Özdemir; Keriman Günaydin; F. Bedia Erim

doi:10.1016/j.talanta.2006.05.018

Analysis of anthraquinones in Rumex crispus by micellar electrokinetic chromatography

Selda Başkan
, Ayşe Daut-Özdemir
, Keriman Günaydin
, F. Bedia Erim^*

^*Bu çalışma için yazışmadan sorumlu yazar

Kimya Bölümü

Araştırma sonucu: Dergiye katkı › Makale › bilirkişi

28 Atıf (Scopus)

Özet

A micellar electrochromatographic method was performed for the analysis of the pharmaceutically important anthraquinones from the root of Rumex crispus. The separation of 1,5-dihydroxy-3-methylanthraquinone (1); 1,3,5-trihydroxy-6-hydroxymethylanthraquinone (2); 1,5-dihydroxy-3-methoxy-7-methylanthraquinone (3) was achieved in 6 min using a running buffer containing 10 mmol/l sodium borate, 50 mmol/l sodium dodecylsulfate, and 25% acetonitrile at pH 10.6. The method is simple, rapid, and reproducible.

Orijinal dil	İngilizce
Sayfa (başlangıç-bitiş)	747-750
Sayfa sayısı	4
Dergi	Talanta
Hacim	71
Basın numarası	2
DOI'lar	https://doi.org/10.1016/j.talanta.2006.05.018
Yayın durumu	Yayınlandı - 15 Şub 2007

Finansman

We thank the TÜBITAK (Grant TBA6-2312, 103T053) for financial support.

Finansörler	Finansör numarası
Türkiye Bilimsel ve Teknolojik Araştirma Kurumu	103T053, TBA6-2312

Belgeye Erişim

10.1016/j.talanta.2006.05.018

Diğer Dosyalar ve Linkler

Link to publication in Scopus

Alıntı Yap

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title = "Analysis of anthraquinones in Rumex crispus by micellar electrokinetic chromatography",

abstract = "A micellar electrochromatographic method was performed for the analysis of the pharmaceutically important anthraquinones from the root of Rumex crispus. The separation of 1,5-dihydroxy-3-methylanthraquinone (1); 1,3,5-trihydroxy-6-hydroxymethylanthraquinone (2); 1,5-dihydroxy-3-methoxy-7-methylanthraquinone (3) was achieved in 6 min using a running buffer containing 10 mmol/l sodium borate, 50 mmol/l sodium dodecylsulfate, and 25\% acetonitrile at pH 10.6. The method is simple, rapid, and reproducible.",

keywords = "Anthraquinones, Capillary electrophoresis, MEKC, Rumex crispus",

author = "Selda Ba{\c s}kan and Ay{\c s}e Daut-{\"O}zdemir and Keriman G{\"u}naydin and Erim, \{F. Bedia\}",

year = "2007",

month = feb,

day = "15",

doi = "10.1016/j.talanta.2006.05.018",

language = "English",

volume = "71",

pages = "747--750",

journal = "Talanta",

issn = "0039-9140",

publisher = "Elsevier B.V.",

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TY - JOUR

T1 - Analysis of anthraquinones in Rumex crispus by micellar electrokinetic chromatography

AU - Başkan, Selda

AU - Daut-Özdemir, Ayşe

AU - Günaydin, Keriman

AU - Erim, F. Bedia

PY - 2007/2/15

Y1 - 2007/2/15

N2 - A micellar electrochromatographic method was performed for the analysis of the pharmaceutically important anthraquinones from the root of Rumex crispus. The separation of 1,5-dihydroxy-3-methylanthraquinone (1); 1,3,5-trihydroxy-6-hydroxymethylanthraquinone (2); 1,5-dihydroxy-3-methoxy-7-methylanthraquinone (3) was achieved in 6 min using a running buffer containing 10 mmol/l sodium borate, 50 mmol/l sodium dodecylsulfate, and 25% acetonitrile at pH 10.6. The method is simple, rapid, and reproducible.

AB - A micellar electrochromatographic method was performed for the analysis of the pharmaceutically important anthraquinones from the root of Rumex crispus. The separation of 1,5-dihydroxy-3-methylanthraquinone (1); 1,3,5-trihydroxy-6-hydroxymethylanthraquinone (2); 1,5-dihydroxy-3-methoxy-7-methylanthraquinone (3) was achieved in 6 min using a running buffer containing 10 mmol/l sodium borate, 50 mmol/l sodium dodecylsulfate, and 25% acetonitrile at pH 10.6. The method is simple, rapid, and reproducible.

KW - Anthraquinones

KW - Capillary electrophoresis

KW - MEKC

KW - Rumex crispus

UR - https://www.scopus.com/pages/publications/33846211484

U2 - 10.1016/j.talanta.2006.05.018

DO - 10.1016/j.talanta.2006.05.018

M3 - Article

AN - SCOPUS:33846211484

SN - 0039-9140

VL - 71

SP - 747

EP - 750

JO - Talanta

JF - Talanta

IS - 2

ER -

Analysis of anthraquinones in Rumex crispus by micellar electrokinetic chromatography

Özet

Finansman

Belgeye Erişim

Diğer Dosyalar ve Linkler

Parmak izi

Alıntı Yap