Amonyum floroborat üretimi ve üretim parametrelerinin belirlenmesi

A. Abdullah Ceyhan; Safiye Bağcı; Orhan Baytar; Ömer Şahin

doi:10.30728/boron.687130

Amonyum floroborat üretimi ve üretim parametrelerinin belirlenmesi

A. Abdullah Ceyhan^*
, Safiye Bağcı
, Orhan Baytar
, Ömer Şahin

^*Bu çalışma için yazışmadan sorumlu yazar

Konya Teknik ÜniversitesiMühendislik ve Doğa Bilimleri FakültesiKimya Mühendisliği Bölümü
Selçuk ÜniversitesiMühendislik ve Mimarlık FakültesiKimya Mühendisliği Bölümü
Siirt ÜniversitesiMühendislik FakültesiKimya Mühendisliği Bölümü

Araştırma sonucu: Dergiye katkı › Makale › bilirkişi

5 Atıf (Scopus)

Özet

In this study, the production parameters of ammonium fluoroborate (NH₄BF₄) synthesis with reaction between boric acid and ammonium hydrogen fluoride were investigated. For this purpose, the effects of parameters such as reactive feeding ratio, reaction temperature, stirring rate, stirrer type, second solvent effect determined separately. Surface morphologies and structural analysis of the crystals obtained after reaction were determined by XRD, FT-IR and SEM analysis respectively. The optimum production conditions were found as reactant feeding rate 1:2, reaction temperature 90 °C, stirring type hot air stirring. Limited oxygen index test results showed that ammonium fluoroborate exhibits excellent flame retardance.

Tercüme edilen katkı başlığı	Ammonium fluoroborate production and determination of production parameters
Orijinal dil	Türkçe
Sayfa (başlangıç-bitiş)	63-72
Sayfa sayısı	10
Dergi	Journal of Boron
Hacim	5
Basın numarası	2
DOI'lar	https://doi.org/10.30728/boron.687130
Yayın durumu	Yayınlandı - 29 Haz 2020
Harici olarak yayınlandı	Evet

Bibliyografik not

Publisher Copyright:
© 2020, Turkish Energy Nuclear and Mining Research Institute. All rights reserved.

Keywords

Ammonium fluoroborate
Ammonium hydrogen fluoride
Boric acid
Boron
Flame retardant

Belgeye Erişim

10.30728/boron.687130

Diğer Dosyalar ve Linkler

Link to publication in Scopus

Alıntı Yap

@article{9073177692514f30baf1633efb926b88,

title = "Amonyum floroborat {\"u}retimi ve {\"u}retim parametrelerinin belirlenmesi",

abstract = "In this study, the production parameters of ammonium fluoroborate (NH4BF4) synthesis with reaction between boric acid and ammonium hydrogen fluoride were investigated. For this purpose, the effects of parameters such as reactive feeding ratio, reaction temperature, stirring rate, stirrer type, second solvent effect determined separately. Surface morphologies and structural analysis of the crystals obtained after reaction were determined by XRD, FT-IR and SEM analysis respectively. The optimum production conditions were found as reactant feeding rate 1:2, reaction temperature 90 °C, stirring type hot air stirring. Limited oxygen index test results showed that ammonium fluoroborate exhibits excellent flame retardance.",

keywords = "Ammonium fluoroborate, Ammonium hydrogen fluoride, Boric acid, Boron, Flame retardant",

author = "\{Abdullah Ceyhan\}, A. and Safiye Bağcı and Orhan Baytar and {\"O}mer {\c S}ahin",

year = "2020",

month = jun,

day = "29",

doi = "10.30728/boron.687130",

language = "T{\"u}rk{\c c}e",

volume = "5",

pages = "63--72",

journal = "Journal of Boron",

issn = "2149-9020",

publisher = "Turkish Energy, Nuclear and Mining Research Agency",

number = "2",

}

TY - JOUR

T1 - Amonyum floroborat üretimi ve üretim parametrelerinin belirlenmesi

AU - Abdullah Ceyhan, A.

AU - Bağcı, Safiye

AU - Baytar, Orhan

AU - Şahin, Ömer

PY - 2020/6/29

Y1 - 2020/6/29

N2 - In this study, the production parameters of ammonium fluoroborate (NH4BF4) synthesis with reaction between boric acid and ammonium hydrogen fluoride were investigated. For this purpose, the effects of parameters such as reactive feeding ratio, reaction temperature, stirring rate, stirrer type, second solvent effect determined separately. Surface morphologies and structural analysis of the crystals obtained after reaction were determined by XRD, FT-IR and SEM analysis respectively. The optimum production conditions were found as reactant feeding rate 1:2, reaction temperature 90 °C, stirring type hot air stirring. Limited oxygen index test results showed that ammonium fluoroborate exhibits excellent flame retardance.

AB - In this study, the production parameters of ammonium fluoroborate (NH4BF4) synthesis with reaction between boric acid and ammonium hydrogen fluoride were investigated. For this purpose, the effects of parameters such as reactive feeding ratio, reaction temperature, stirring rate, stirrer type, second solvent effect determined separately. Surface morphologies and structural analysis of the crystals obtained after reaction were determined by XRD, FT-IR and SEM analysis respectively. The optimum production conditions were found as reactant feeding rate 1:2, reaction temperature 90 °C, stirring type hot air stirring. Limited oxygen index test results showed that ammonium fluoroborate exhibits excellent flame retardance.

KW - Ammonium fluoroborate

KW - Ammonium hydrogen fluoride

KW - Boric acid

KW - Boron

KW - Flame retardant

UR - https://www.scopus.com/pages/publications/85117698545

U2 - 10.30728/boron.687130

DO - 10.30728/boron.687130

M3 - Makale

AN - SCOPUS:85117698545

SN - 2149-9020

VL - 5

SP - 63

EP - 72

JO - Journal of Boron

JF - Journal of Boron

IS - 2

ER -

Amonyum floroborat üretimi ve üretim parametrelerinin belirlenmesi

Özet

Bibliyografik not

Keywords

Belgeye Erişim

Diğer Dosyalar ve Linkler

Parmak izi

Alıntı Yap