Time-resolved grazing-incidence X-ray diffraction measurement to understand the effect of hydrogen on surface strain development in super duplex stainless steel

Cem Örnek; Alfred Larsson; Gary S. Harlow; Fan Zhang; Robin Kroll; Franceso Carlà; Hadeel Hussain; Ulf Kivisäkk; Dirk L. Engelberg; Edvin Lundgren; Jinshan Pan

doi:10.1016/j.scriptamat.2020.05.061

Time-resolved grazing-incidence X-ray diffraction measurement to understand the effect of hydrogen on surface strain development in super duplex stainless steel

Cem Örnek
, Alfred Larsson
, Gary S. Harlow
, Fan Zhang
, Robin Kroll
, Franceso Carlà
, Hadeel Hussain
, Ulf Kivisäkk
, Dirk L. Engelberg
, Edvin Lundgren
, Jinshan Pan^*

^*Corresponding author for this work

Department of Metallurgical and Materials Engineering

KTH Royal Institute of Technology
Lund University
University of Manchester
Diamond Light Source
Sandvik AB

Research output: Contribution to journal › Article › peer-review

12 Citations (Scopus)

Abstract

Grazing-incidence x-ray diffraction was employed to measure, operando, during electrochemical hydrogen charging, the lattice strain development of the near-surface in super duplex stainless steel under applied tensile load. Hydrogen absorption led to the formation of tensile strains in both the austenite (γ) and ferrite (δ) phases perpendicular to the loading axis, whereas compressive strains were formed in the ferrite phase parallel to the loading direction, despite the acting tensile load. The earliest stages of degradation are discussed in light of understanding hydrogen embrittlement.

Original language	English
Pages (from-to)	63-67
Number of pages	5
Journal	Scripta Materialia
Volume	187
DOIs	https://doi.org/10.1016/j.scriptamat.2020.05.061
Publication status	Published - Oct 2020

Bibliographical note

Publisher Copyright:
© 2020 Acta Materialia Inc. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/)

Keywords

Dual phases
Hydrogen embrittlement
Stainless steels
Synchrotron radiation
X-ray diffraction (XRD)

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10.1016/j.scriptamat.2020.05.061

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Örnek, C., Larsson, A., Harlow, G. S., Zhang, F., Kroll, R., Carlà, F., Hussain, H., Kivisäkk, U., Engelberg, D. L., Lundgren, E., & Pan, J. (2020). Time-resolved grazing-incidence X-ray diffraction measurement to understand the effect of hydrogen on surface strain development in super duplex stainless steel. Scripta Materialia, 187, 63-67. https://doi.org/10.1016/j.scriptamat.2020.05.061

@article{33bc8c7381df4237af65510d25bcd846,

title = "Time-resolved grazing-incidence X-ray diffraction measurement to understand the effect of hydrogen on surface strain development in super duplex stainless steel",

abstract = "Grazing-incidence x-ray diffraction was employed to measure, operando, during electrochemical hydrogen charging, the lattice strain development of the near-surface in super duplex stainless steel under applied tensile load. Hydrogen absorption led to the formation of tensile strains in both the austenite (γ) and ferrite (δ) phases perpendicular to the loading axis, whereas compressive strains were formed in the ferrite phase parallel to the loading direction, despite the acting tensile load. The earliest stages of degradation are discussed in light of understanding hydrogen embrittlement.",

keywords = "Dual phases, Hydrogen embrittlement, Stainless steels, Synchrotron radiation, X-ray diffraction (XRD)",

author = "Cem {\"O}rnek and Alfred Larsson and Harlow, \{Gary S.\} and Fan Zhang and Robin Kroll and Franceso Carl{\`a} and Hadeel Hussain and Ulf Kivis{\"a}kk and Engelberg, \{Dirk L.\} and Edvin Lundgren and Jinshan Pan",

note = "Publisher Copyright: {\textcopyright} 2020 Acta Materialia Inc. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/)",

year = "2020",

month = oct,

doi = "10.1016/j.scriptamat.2020.05.061",

language = "English",

volume = "187",

pages = "63--67",

journal = "Scripta Materialia",

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}

Örnek, C, Larsson, A, Harlow, GS, Zhang, F, Kroll, R, Carlà, F, Hussain, H, Kivisäkk, U, Engelberg, DL, Lundgren, E & Pan, J 2020, 'Time-resolved grazing-incidence X-ray diffraction measurement to understand the effect of hydrogen on surface strain development in super duplex stainless steel', Scripta Materialia, vol. 187, pp. 63-67. https://doi.org/10.1016/j.scriptamat.2020.05.061

TY - JOUR

T1 - Time-resolved grazing-incidence X-ray diffraction measurement to understand the effect of hydrogen on surface strain development in super duplex stainless steel

AU - Örnek, Cem

AU - Larsson, Alfred

AU - Harlow, Gary S.

AU - Zhang, Fan

AU - Kroll, Robin

AU - Carlà, Franceso

AU - Hussain, Hadeel

AU - Kivisäkk, Ulf

AU - Engelberg, Dirk L.

AU - Lundgren, Edvin

AU - Pan, Jinshan

PY - 2020/10

Y1 - 2020/10

N2 - Grazing-incidence x-ray diffraction was employed to measure, operando, during electrochemical hydrogen charging, the lattice strain development of the near-surface in super duplex stainless steel under applied tensile load. Hydrogen absorption led to the formation of tensile strains in both the austenite (γ) and ferrite (δ) phases perpendicular to the loading axis, whereas compressive strains were formed in the ferrite phase parallel to the loading direction, despite the acting tensile load. The earliest stages of degradation are discussed in light of understanding hydrogen embrittlement.

AB - Grazing-incidence x-ray diffraction was employed to measure, operando, during electrochemical hydrogen charging, the lattice strain development of the near-surface in super duplex stainless steel under applied tensile load. Hydrogen absorption led to the formation of tensile strains in both the austenite (γ) and ferrite (δ) phases perpendicular to the loading axis, whereas compressive strains were formed in the ferrite phase parallel to the loading direction, despite the acting tensile load. The earliest stages of degradation are discussed in light of understanding hydrogen embrittlement.

KW - Dual phases

KW - Hydrogen embrittlement

KW - Stainless steels

KW - Synchrotron radiation

KW - X-ray diffraction (XRD)

UR - https://www.scopus.com/pages/publications/85086398345

U2 - 10.1016/j.scriptamat.2020.05.061

DO - 10.1016/j.scriptamat.2020.05.061

M3 - Article

AN - SCOPUS:85086398345

SN - 1359-6462

VL - 187

SP - 63

EP - 67

JO - Scripta Materialia

JF - Scripta Materialia

ER -

Time-resolved grazing-incidence X-ray diffraction measurement to understand the effect of hydrogen on surface strain development in super duplex stainless steel

Abstract

Bibliographical note

Keywords

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