TY - GEN
T1 - Synthesis of nanocrystalline lead oxide particles by ultrasonic spray pyrolysis method
AU - Ebin, Burcak
AU - Gurmen, Sebahattin
AU - Arslan, Cuneyt
PY - 2010
Y1 - 2010
N2 - Lead oxide is a very important metal oxide semiconductor and considerable progresses have been made in the study of the production and applications such as in storage battaries, gas sensors and pigments. Nanocrystalline lead oxide particles were synthesized by ultrasonic spray pyrolysis method (USP) using lead nitrate solution under air flow rate at 600°C. Characterization studies of the nanocrystalline particles conducted on not only size and shape morphology of the particles, but also chemical composition, phase determination, crystal size, and band gap energy of the particles by the help of scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and UV-vis spectrophotometer. Analyses show that spherical PbO particles are in submicron range, and otherwise their crystalline size was determined 38 nm using Scherrer formulation.
AB - Lead oxide is a very important metal oxide semiconductor and considerable progresses have been made in the study of the production and applications such as in storage battaries, gas sensors and pigments. Nanocrystalline lead oxide particles were synthesized by ultrasonic spray pyrolysis method (USP) using lead nitrate solution under air flow rate at 600°C. Characterization studies of the nanocrystalline particles conducted on not only size and shape morphology of the particles, but also chemical composition, phase determination, crystal size, and band gap energy of the particles by the help of scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and UV-vis spectrophotometer. Analyses show that spherical PbO particles are in submicron range, and otherwise their crystalline size was determined 38 nm using Scherrer formulation.
KW - Lead oxide
KW - Particle
KW - Ultrasonic spray pyrolysis
UR - http://www.scopus.com/inward/record.url?scp=84902138268&partnerID=8YFLogxK
M3 - Conference contribution
AN - SCOPUS:84902138268
SN - 9781899072194
T3 - Proceedings of the World Powder Metallurgy Congress and Exhibition, World PM 2010
BT - Proceedings of the World Powder Metallurgy Congress and Exhibition, World PM 2010
PB - European Powder Metallurgy Association (EPMA)
T2 - World Powder Metallurgy Congress and Exhibition, World PM 2010
Y2 - 10 October 2010 through 14 October 2010
ER -