Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

Kagan Benzesik; Filiz Çınar Şahin; Onuralp Yücel

doi:10.1007/978-3-031-80748-0_108

Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

Kagan Benzesik^*, Filiz Çınar Şahin, Onuralp Yücel

^*Corresponding author for this work

Department of Metallurgical and Materials Engineering

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

In this study, the SPS conditions of Li₄SiO₄ powders produced by combustion synthesis were investigated. There is no study on the sintering of Li₄SiO₄ powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.

Original language	English
Title of host publication	TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings
Publisher	Springer Science and Business Media Deutschland GmbH
Pages	1217-1226
Number of pages	10
ISBN (Print)	9783031807473
DOIs	https://doi.org/10.1007/978-3-031-80748-0_108
Publication status	Published - 2025
Event	154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025 - Las Vegas, United States Duration: 23 Mar 2025 → 27 Mar 2025

Publication series

Name	Minerals, Metals and Materials Series
ISSN (Print)	2367-1181
ISSN (Electronic)	2367-1696

Conference

Conference	154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025
Country/Territory	United States
City	Las Vegas
Period	23/03/25 → 27/03/25

Bibliographical note

Publisher Copyright:
© The Minerals, Metals & Materials Society 2025.

Keywords

Compaction
Spark plasma sintering
Tritium breeding

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

Access to Document

10.1007/978-3-031-80748-0_108

Cite this

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title = "Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders",

abstract = "In this study, the SPS conditions of Li4SiO4 powders produced by combustion synthesis were investigated. There is no study on the sintering of Li4SiO4 powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100\%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.",

keywords = "Compaction, Spark plasma sintering, Tritium breeding",

author = "Kagan Benzesik and {\c S}ahin, \{Filiz {\c C}ınar\} and Onuralp Y{\"u}cel",

note = "Publisher Copyright: {\textcopyright} The Minerals, Metals \& Materials Society 2025.; 154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025 ; Conference date: 23-03-2025 Through 27-03-2025",

year = "2025",

doi = "10.1007/978-3-031-80748-0\_108",

language = "English",

isbn = "9783031807473",

series = "Minerals, Metals and Materials Series",

publisher = "Springer Science and Business Media Deutschland GmbH",

pages = "1217--1226",

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address = "Germany",

}

Benzesik, K , Şahin, FÇ & Yücel, O 2025, Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders. in TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings. Minerals, Metals and Materials Series, Springer Science and Business Media Deutschland GmbH, pp. 1217-1226, 154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025, Las Vegas, United States, 23/03/25. https://doi.org/10.1007/978-3-031-80748-0_108

Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders. / Benzesik, Kagan ; Şahin, Filiz Çınar ; Yücel, Onuralp.
TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings. Springer Science and Business Media Deutschland GmbH, 2025. p. 1217-1226 (Minerals, Metals and Materials Series).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

AU - Benzesik, Kagan

AU - Şahin, Filiz Çınar

AU - Yücel, Onuralp

PY - 2025

Y1 - 2025

N2 - In this study, the SPS conditions of Li4SiO4 powders produced by combustion synthesis were investigated. There is no study on the sintering of Li4SiO4 powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.

AB - In this study, the SPS conditions of Li4SiO4 powders produced by combustion synthesis were investigated. There is no study on the sintering of Li4SiO4 powders with SPS in the literature. Therefore, this study has made an innovative contribution to the literature. The combustion synthesis products were first ground by hand in an agate mortar. Then, the powders were placed in a graphite mold and pre-pressure of 10 MPa was applied with the help of an axial hydraulic press. In this way, it was aimed to obtain a compact product with a theoretical density of 100%, a diameter of 50 mm, and a thickness of 5 mm. The mold was then wrapped with a graphite blanket and placed inside the sintering chamber. All SPS experiments were conducted in a vacuum atmosphere. For each experiment, the heating rate was set at 100 °C/min and the sintering time was 5 min.

KW - Compaction

KW - Spark plasma sintering

KW - Tritium breeding

UR - https://www.scopus.com/pages/publications/105003993406

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DO - 10.1007/978-3-031-80748-0_108

M3 - Conference contribution

AN - SCOPUS:105003993406

SN - 9783031807473

T3 - Minerals, Metals and Materials Series

SP - 1217

EP - 1226

BT - TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings

PB - Springer Science and Business Media Deutschland GmbH

T2 - 154th Annual Meeting and Exhibition of The Minerals, Metals and Materials Society, TMS 2025

Y2 - 23 March 2025 through 27 March 2025

ER -

Spark Plasma Sintering of Combustion Synthesis-Derived Lithium Orthosilicate Powders

Abstract

Publication series

Conference

Bibliographical note

Keywords

UN SDGs

Access to Document

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