Polymers with acyloxime ester groups in the main chain. 2. Photochemical synthesis of block copolymers

Tülin İmamoǧlu; Ayşen Önen; Yusuf Yaǧci

doi:10.1002/apmc.1995.052240115

Polymers with acyloxime ester groups in the main chain. 2. Photochemical synthesis of block copolymers

Tülin İmamoǧlu
, Ayşen Önen
, Yusuf Yaǧci^*

^*Corresponding author for this work

Department of Chemistry

Istanbul Technical University

Research output: Contribution to journal › Article › peer-review

7 Citations (Scopus)

Abstract

Block copolymers of styrene and methyl methacrylate (MMA) were prepared in a two‐stage free‐radical polymerization by means of an azo‐acyloxime ester (AOE) initiator. In the first stage, photosensitive styrene prepolymers were synthesized by using AOE initiator. These polymers were photolysed in the presence of MMA in the second stage to form block copolymers. The block copolymer structure was elucidated by means of extraction by appropriate solvents, GPC analysis and IR and NMR spectral measurements.

Original language	English
Pages (from-to)	145-151
Number of pages	7
Journal	Angewandte Makromolekulare Chemie
Volume	224
Issue number	1
DOIs	https://doi.org/10.1002/apmc.1995.052240115
Publication status	Published - Jan 1995

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abstract = "Block copolymers of styrene and methyl methacrylate (MMA) were prepared in a two‐stage free‐radical polymerization by means of an azo‐acyloxime ester (AOE) initiator. In the first stage, photosensitive styrene prepolymers were synthesized by using AOE initiator. These polymers were photolysed in the presence of MMA in the second stage to form block copolymers. The block copolymer structure was elucidated by means of extraction by appropriate solvents, GPC analysis and IR and NMR spectral measurements.",

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AU - İmamoǧlu, Tülin

AU - Önen, Ayşen

AU - Yaǧci, Yusuf

PY - 1995/1

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N2 - Block copolymers of styrene and methyl methacrylate (MMA) were prepared in a two‐stage free‐radical polymerization by means of an azo‐acyloxime ester (AOE) initiator. In the first stage, photosensitive styrene prepolymers were synthesized by using AOE initiator. These polymers were photolysed in the presence of MMA in the second stage to form block copolymers. The block copolymer structure was elucidated by means of extraction by appropriate solvents, GPC analysis and IR and NMR spectral measurements.

AB - Block copolymers of styrene and methyl methacrylate (MMA) were prepared in a two‐stage free‐radical polymerization by means of an azo‐acyloxime ester (AOE) initiator. In the first stage, photosensitive styrene prepolymers were synthesized by using AOE initiator. These polymers were photolysed in the presence of MMA in the second stage to form block copolymers. The block copolymer structure was elucidated by means of extraction by appropriate solvents, GPC analysis and IR and NMR spectral measurements.

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U2 - 10.1002/apmc.1995.052240115

DO - 10.1002/apmc.1995.052240115

M3 - Article

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Polymers with acyloxime ester groups in the main chain. 2. Photochemical synthesis of block copolymers

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