Monitoring of oil-based polyurethane synthesis by FTIR-ATR

Hande Madra; S. Birgul Tantekin-Ersolmaz; F. Seniha Guner

doi:10.1016/j.polymertesting.2009.05.013

Monitoring of oil-based polyurethane synthesis by FTIR-ATR

Hande Madra
, S. Birgul Tantekin-Ersolmaz
, F. Seniha Guner^*

^*Corresponding author for this work

Department of Chemical Engineering

Istanbul Technical University

Research output: Contribution to journal › Article › peer-review

33 Citations (Scopus)

Abstract

Oil-based polyurethanes were synthesized from triglyceride oil-based hydroxyl containing material and toluene diisocyanate or hexamethylene diisocyanate for wound dressing applications. The reactions were carried out with or without catalyst at 90 °C. The amount of free isocyanate during the reaction was determined by a FTIR-ATR method, and the results were compared with those from a back-titration method. The data obtained were used for determination of kinetic parameters.

Original language	English
Pages (from-to)	773-779
Number of pages	7
Journal	Polymer Testing
Volume	28
Issue number	7
DOIs	https://doi.org/10.1016/j.polymertesting.2009.05.013
Publication status	Published - Oct 2009

Keywords

FTIR-ATR
Polyurethane
Triglyceride oil

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10.1016/j.polymertesting.2009.05.013

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abstract = "Oil-based polyurethanes were synthesized from triglyceride oil-based hydroxyl containing material and toluene diisocyanate or hexamethylene diisocyanate for wound dressing applications. The reactions were carried out with or without catalyst at 90 °C. The amount of free isocyanate during the reaction was determined by a FTIR-ATR method, and the results were compared with those from a back-titration method. The data obtained were used for determination of kinetic parameters.",

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AU - Madra, Hande

AU - Tantekin-Ersolmaz, S. Birgul

AU - Guner, F. Seniha

PY - 2009/10

Y1 - 2009/10

N2 - Oil-based polyurethanes were synthesized from triglyceride oil-based hydroxyl containing material and toluene diisocyanate or hexamethylene diisocyanate for wound dressing applications. The reactions were carried out with or without catalyst at 90 °C. The amount of free isocyanate during the reaction was determined by a FTIR-ATR method, and the results were compared with those from a back-titration method. The data obtained were used for determination of kinetic parameters.

AB - Oil-based polyurethanes were synthesized from triglyceride oil-based hydroxyl containing material and toluene diisocyanate or hexamethylene diisocyanate for wound dressing applications. The reactions were carried out with or without catalyst at 90 °C. The amount of free isocyanate during the reaction was determined by a FTIR-ATR method, and the results were compared with those from a back-titration method. The data obtained were used for determination of kinetic parameters.

KW - FTIR-ATR

KW - Polyurethane

KW - Triglyceride oil

UR - https://www.scopus.com/pages/publications/68549126752

U2 - 10.1016/j.polymertesting.2009.05.013

DO - 10.1016/j.polymertesting.2009.05.013

M3 - Article

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SP - 773

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ER -

Monitoring of oil-based polyurethane synthesis by FTIR-ATR

Abstract

Keywords

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