TY - GEN
T1 - Iron-nickel-cobalt (Fe-Ni-Co) alloy particles prepared by ultrasonic spray pyrolysis and hydrogen reduction (USP-HR) method
AU - Toparli, Cigdem
AU - Ebin, Burcak
AU - Gürmen, Sebahattin
PY - 2013
Y1 - 2013
N2 - Nanocrystalline FeNiCo ternary alloy particles were synthesized by ultrasonic spray pyrolysis and hydrogen reduction method. Fe(NO 3)3.9H2O, Ni(NO3) 2.6H2O and Co(NO3)2.6H2O were used as a starting material to synthesize the nanocrystalline spherical ternary alloy particles. The experiments were performed at 600, 800 and 1000°C using iron-nickel-cobalt nitrate aqueous solution. Shape, morphology, size, chemical composition and crystal structure of the particles were investigated. X-ray diffraction (XRD), scanning electron microscope (FEG-SEM) and energy dispersive spectroscopy (EDS) studies were carried out to characterize the ternary alloys particles. Vibrating sample magnetometer (VSM) was used to characterize the magnetic properties. Spherical nanocrystalline FeNiCo ternary alloy particles were prepared in the size range of 65 and 500 nm. Average crystallite size of the particles is 50 nm.
AB - Nanocrystalline FeNiCo ternary alloy particles were synthesized by ultrasonic spray pyrolysis and hydrogen reduction method. Fe(NO 3)3.9H2O, Ni(NO3) 2.6H2O and Co(NO3)2.6H2O were used as a starting material to synthesize the nanocrystalline spherical ternary alloy particles. The experiments were performed at 600, 800 and 1000°C using iron-nickel-cobalt nitrate aqueous solution. Shape, morphology, size, chemical composition and crystal structure of the particles were investigated. X-ray diffraction (XRD), scanning electron microscope (FEG-SEM) and energy dispersive spectroscopy (EDS) studies were carried out to characterize the ternary alloys particles. Vibrating sample magnetometer (VSM) was used to characterize the magnetic properties. Spherical nanocrystalline FeNiCo ternary alloy particles were prepared in the size range of 65 and 500 nm. Average crystallite size of the particles is 50 nm.
UR - http://www.scopus.com/inward/record.url?scp=84880908515&partnerID=8YFLogxK
M3 - Conference contribution
AN - SCOPUS:84880908515
SN - 9781118744093
T3 - Ceramic Transactions
SP - 247
EP - 254
BT - Processing and Properties of Advanced Ceramics and Composites V
T2 - Processing and Properties of Advanced Ceramics and Composites V - Materials Science and Technology 2012 Conference, MS and T 2012
Y2 - 7 October 2012 through 12 October 2012
ER -