In situ synthesis of B4C/TiB2 composites from low cost sugar based precursor

E. Çakir; C. Ergun; F. Ç Şahin; I. Erden

doi:10.4028/www.scientific.net/DDF.297-301.52

In situ synthesis of B₄C/TiB₂ composites from low cost sugar based precursor

E. Çakir^*, C. Ergun, F. Ç Şahin, I. Erden

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

9 Citations (Scopus)

Abstract

In the present study, a method based on sulfuric acid dehydration of sugar was developed to synthesis a precursor material, which can yield B ₄C/TiB₂ composites at much lower temperatures compared to traditional carbothermal methods. The precursor material for pure B₄C and B₄C/TiB₂ composites were heat treated at 1650°C under Ar and Ar+H₂ atmosphere. Then the samples were characterized by X-ray diffraction (XRD) and crystallized B₄C and B ₄C/TiB₂ composites can be obtained at 1650°C.

Original language	English
Title of host publication	Diffusion in Solids and Liquids V
Publisher	Trans Tech Publications Ltd
Pages	52-56
Number of pages	5
Volume	297-301
ISBN (Print)	3908451809, 9783908451808
DOIs	https://doi.org/10.4028/www.scientific.net/DDF.297-301.52
Publication status	Published - 2010

Keywords

Boron carbide
Ceramic precursor
Ceramic synthesis
Low temperature synthesis
Titanium diboride

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10.4028/www.scientific.net/DDF.297-301.52

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title = "In situ synthesis of B4C/TiB2 composites from low cost sugar based precursor",

abstract = "In the present study, a method based on sulfuric acid dehydration of sugar was developed to synthesis a precursor material, which can yield B 4C/TiB2 composites at much lower temperatures compared to traditional carbothermal methods. The precursor material for pure B4C and B4C/TiB2 composites were heat treated at 1650°C under Ar and Ar+H2 atmosphere. Then the samples were characterized by X-ray diffraction (XRD) and crystallized B4C and B 4C/TiB2 composites can be obtained at 1650°C.",

keywords = "Boron carbide, Ceramic precursor, Ceramic synthesis, Low temperature synthesis, Titanium diboride",

author = "E. {\c C}akir and C. Ergun and {\c S}ahin, {F. {\c C}} and I. Erden",

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language = "English",

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T1 - In situ synthesis of B4C/TiB2 composites from low cost sugar based precursor

AU - Çakir, E.

AU - Ergun, C.

AU - Şahin, F. Ç

AU - Erden, I.

PY - 2010

Y1 - 2010

N2 - In the present study, a method based on sulfuric acid dehydration of sugar was developed to synthesis a precursor material, which can yield B 4C/TiB2 composites at much lower temperatures compared to traditional carbothermal methods. The precursor material for pure B4C and B4C/TiB2 composites were heat treated at 1650°C under Ar and Ar+H2 atmosphere. Then the samples were characterized by X-ray diffraction (XRD) and crystallized B4C and B 4C/TiB2 composites can be obtained at 1650°C.

AB - In the present study, a method based on sulfuric acid dehydration of sugar was developed to synthesis a precursor material, which can yield B 4C/TiB2 composites at much lower temperatures compared to traditional carbothermal methods. The precursor material for pure B4C and B4C/TiB2 composites were heat treated at 1650°C under Ar and Ar+H2 atmosphere. Then the samples were characterized by X-ray diffraction (XRD) and crystallized B4C and B 4C/TiB2 composites can be obtained at 1650°C.

KW - Boron carbide

KW - Ceramic precursor

KW - Ceramic synthesis

KW - Low temperature synthesis

KW - Titanium diboride

UR - http://www.scopus.com/inward/record.url?scp=77952259211&partnerID=8YFLogxK

U2 - 10.4028/www.scientific.net/DDF.297-301.52

DO - 10.4028/www.scientific.net/DDF.297-301.52

M3 - Conference contribution

AN - SCOPUS:77952259211

SN - 3908451809

SN - 9783908451808

VL - 297-301

SP - 52

EP - 56

BT - Diffusion in Solids and Liquids V

PB - Trans Tech Publications Ltd

ER -

In situ synthesis of B₄C/TiB₂ composites from low cost sugar based precursor

Abstract

Keywords

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