Identification of cracks generated by indentation experiments in hard-coating systems

M. K. Kazmanli*, B. Rother, M. Ürgen, C. Mitterer

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

17 Citations (Scopus)

Abstract

In this work, depth-sensing indentation measurements were applied to Zr-B-N and Zr-B monolayers as well as to multilayer systems of the same materials (two-, four- and 16-layer samples). The coatings were deposited on to Ck 35 carbon steels by reactive (Zr-B-N) and non-reactive (Zr-B) d.c. magnetron sputtering. Crack-formation processes during the penetration of the indenter were examined by analysis of the load-indentation data and by scanning electron microscopy (SEM). The analysis of the load-indentation data was performed by using averaging, smoothing and numerical differentiation procedures. Correlations between the results of the data analysis and the SEM observations are outlined, and the advantages of multilayer systems are demonstrated.

Original languageEnglish
Pages (from-to)65-75
Number of pages11
JournalSurface and Coatings Technology
Volume107
Issue number1
DOIs
Publication statusPublished - 21 Aug 1998

Funding

The authors gratefully acknowledge the contribution of NATO SfS TU-PVD Coatings Project and Prof. Dr Ali Fuat Çakir (project director) to this work by supplying financial support to Mr K. Kazmanli during his stay at FEM. Parts of the work were supported by the German Federal Ministry for Economic Affairs and the Association of Industrial Research Alliances under contract number AiF 10499N.

FundersFunder number
Association of Industrial Research AlliancesAiF 10499N
German Federal Ministry for Economic Affairs
North Atlantic Treaty Organization

    Keywords

    • Depth-sensing indentation
    • Hard-coating systems
    • Zr-B
    • Zr-B-N

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