Highly efficient and selective heterogeneous catalytic reduction of 2-nitroaniline by cerium oxide nanocatalyst under microwave irradiation

Efficient nanocatalyst with incredible performance is highly demanding in a heterogeneous catalysis system. Herein, we report the facile fabrication of uniform and highly stable Cerium Oxide nanoparticles (CeO₂ NPs), through chemical precipitation method using sodium hydroxide as reducing agent. The synthesized material is characterized through highly sophisticated techniques including UV-Visible, FT-IR, SEM, AFM, XRD, and Zeta Sizer- Potential to check the particle formation, surface morphology, topography, crystalline nature, size, and surface potential. The heterogeneous catalytic performance of CeO₂ NPs has been accomplished for the reduction of 2-nitroaniline from the aqueous media. The CeO₂ nanocatalyst displayed excellent reusability, while the reduction in several repetitive catalytic cycles against 2-nitroaniline under optimized conditions. The CeO₂ nanocatalyst shows 99.12% efficiency within 60s reaction time under a greener source of microwave radiation.