Effect of Different Parameters on Membrane Concentrate Treatment by using Vacuum Assisted Air Gap Membrane Distillation Crystallization (VAGMD-C)

Oyku Mutlu-Salmanli, Ismail Koyuncu*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

Abstract

The concentration problem represents a significant challenge for membrane processes, necessitating supplementary treatment and management strategies. This study assesses the efficiency of a vacuum-assisted air gap membrane distillation/crystallization (VAGMD-C) system to addressing this issue, specifically focusing on the removal and recovery of boron, a critical raw material. Synthetic boron solutions were employed to optimize key parameters such as concentration, pH, and membrane type. Following this, real reverse osmosis (RO) concentrate was treated under optimized conditions using both commercial and custom-fabricated membranes. The experimental analyses included flux measurements, boron concentration assessments, and boron rejection rates, along with scanning electron microscope-energy dispersive spectrometry (SEM–EDS) and X-ray fluorescence (XRF) analysis of the resulting crystals. The results demonstrated that achieving up to 44.6% boron content in the crystals is feasible by utilizing the fabricated nanofiber membrane (NF) within the VAGMD-C system.

Original languageEnglish
Article number321
JournalWater, Air, and Soil Pollution
Volume236
Issue number5
DOIs
Publication statusPublished - May 2025

Bibliographical note

Publisher Copyright:
© The Author(s) 2025.

Keywords

  • Boron
  • Concentrate treatment
  • Crystallization
  • Membrane distillation
  • Resource recovery

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