Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles

Ramazan Oguzhan Apaydin; Burcak Ebin; Sebahattin Gurmen

doi:10.1063/1.4849228

Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles

Ramazan Oguzhan Apaydin, Burcak Ebin, Sebahattin Gurmen

Department of Metallurgical and Materials Engineering

Istanbul Technical University

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

2 Citations (Scopus)

Abstract

Copper-Nickel (CuNi) nanostructured alloy particles were produced by Ultrasonic Spray Pyrolysis and Hydrogen Reduction Method (USP-HR) from high purity copper and nickel nitrate aqueous solutions. The effect of the precursor solution in the range of 0.1 and 0.5 mol/L on the morphology and crystallite size of CuNi nanoparticles were investigated under 2 h running time, 700 °C operating temperature and 0.5 L/min H2 flow rate. Particle size, morphology, composition and crystallite structure were characterized by Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS) and X-Ray Diffraction (XRD). Particle characterization studies show that nanostructured alloy particles have cubic crystal structure and they are in submicron size range with spherical morphology. The crystallite sizes of the particles calculated with Scherrer formula are 40 and 34 nm and average particles sizes observed from the SEM images are 300 and 510 nm for each experiment respectively.

Original language	English
Title of host publication	3rd International Advances in Applied Physics and Materials Science Congress
Editors	Asli Sonmez, Zehra Banu Bahsi, Ahmet Yavuz Oral
Publisher	American Institute of Physics Inc.
Pages	57-60
Number of pages	4
ISBN (Electronic)	9780735411975
DOIs	https://doi.org/10.1063/1.4849228
Publication status	Published - 2013
Event	3rd International Advances in Applied Physics and Materials Science Congress, APMAS 2013 - Antalya, Turkey Duration: 24 Apr 2013 → 28 Apr 2013

Publication series

Name	AIP Conference Proceedings
Volume	1569
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	3rd International Advances in Applied Physics and Materials Science Congress, APMAS 2013
Country/Territory	Turkey
City	Antalya
Period	24/04/13 → 28/04/13

Bibliographical note

Publisher Copyright:
© 2013 AIP Publishing LLC.

Keywords

alloy particle
copper nickel
hydrogen reduction
nanocrystallite
ultrasonic spray pyrolysis

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10.1063/1.4849228

Cite this

Apaydin, R. O., Ebin, B., & Gurmen, S. (2013). Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles. In A. Sonmez, Z. B. Bahsi, & A. Y. Oral (Eds.), 3rd International Advances in Applied Physics and Materials Science Congress (pp. 57-60). (AIP Conference Proceedings; Vol. 1569). American Institute of Physics Inc.. https://doi.org/10.1063/1.4849228

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title = "Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles",

abstract = "Copper-Nickel (CuNi) nanostructured alloy particles were produced by Ultrasonic Spray Pyrolysis and Hydrogen Reduction Method (USP-HR) from high purity copper and nickel nitrate aqueous solutions. The effect of the precursor solution in the range of 0.1 and 0.5 mol/L on the morphology and crystallite size of CuNi nanoparticles were investigated under 2 h running time, 700 °C operating temperature and 0.5 L/min H2 flow rate. Particle size, morphology, composition and crystallite structure were characterized by Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS) and X-Ray Diffraction (XRD). Particle characterization studies show that nanostructured alloy particles have cubic crystal structure and they are in submicron size range with spherical morphology. The crystallite sizes of the particles calculated with Scherrer formula are 40 and 34 nm and average particles sizes observed from the SEM images are 300 and 510 nm for each experiment respectively.",

keywords = "alloy particle, copper nickel, hydrogen reduction, nanocrystallite, ultrasonic spray pyrolysis",

author = "Apaydin, {Ramazan Oguzhan} and Burcak Ebin and Sebahattin Gurmen",

note = "Publisher Copyright: {\textcopyright} 2013 AIP Publishing LLC.; 3rd International Advances in Applied Physics and Materials Science Congress, APMAS 2013 ; Conference date: 24-04-2013 Through 28-04-2013",

year = "2013",

doi = "10.1063/1.4849228",

language = "English",

series = "AIP Conference Proceedings",

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Apaydin, RO, Ebin, B & Gurmen, S 2013, Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles. in A Sonmez, ZB Bahsi & AY Oral (eds), 3rd International Advances in Applied Physics and Materials Science Congress. AIP Conference Proceedings, vol. 1569, American Institute of Physics Inc., pp. 57-60, 3rd International Advances in Applied Physics and Materials Science Congress, APMAS 2013, Antalya, Turkey, 24/04/13. https://doi.org/10.1063/1.4849228

Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles. / Apaydin, Ramazan Oguzhan; Ebin, Burcak; Gurmen, Sebahattin.
3rd International Advances in Applied Physics and Materials Science Congress. ed. / Asli Sonmez; Zehra Banu Bahsi; Ahmet Yavuz Oral. American Institute of Physics Inc., 2013. p. 57-60 (AIP Conference Proceedings; Vol. 1569).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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T1 - Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles

AU - Apaydin, Ramazan Oguzhan

AU - Ebin, Burcak

AU - Gurmen, Sebahattin

PY - 2013

Y1 - 2013

N2 - Copper-Nickel (CuNi) nanostructured alloy particles were produced by Ultrasonic Spray Pyrolysis and Hydrogen Reduction Method (USP-HR) from high purity copper and nickel nitrate aqueous solutions. The effect of the precursor solution in the range of 0.1 and 0.5 mol/L on the morphology and crystallite size of CuNi nanoparticles were investigated under 2 h running time, 700 °C operating temperature and 0.5 L/min H2 flow rate. Particle size, morphology, composition and crystallite structure were characterized by Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS) and X-Ray Diffraction (XRD). Particle characterization studies show that nanostructured alloy particles have cubic crystal structure and they are in submicron size range with spherical morphology. The crystallite sizes of the particles calculated with Scherrer formula are 40 and 34 nm and average particles sizes observed from the SEM images are 300 and 510 nm for each experiment respectively.

AB - Copper-Nickel (CuNi) nanostructured alloy particles were produced by Ultrasonic Spray Pyrolysis and Hydrogen Reduction Method (USP-HR) from high purity copper and nickel nitrate aqueous solutions. The effect of the precursor solution in the range of 0.1 and 0.5 mol/L on the morphology and crystallite size of CuNi nanoparticles were investigated under 2 h running time, 700 °C operating temperature and 0.5 L/min H2 flow rate. Particle size, morphology, composition and crystallite structure were characterized by Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS) and X-Ray Diffraction (XRD). Particle characterization studies show that nanostructured alloy particles have cubic crystal structure and they are in submicron size range with spherical morphology. The crystallite sizes of the particles calculated with Scherrer formula are 40 and 34 nm and average particles sizes observed from the SEM images are 300 and 510 nm for each experiment respectively.

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KW - copper nickel

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KW - nanocrystallite

KW - ultrasonic spray pyrolysis

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T2 - 3rd International Advances in Applied Physics and Materials Science Congress, APMAS 2013

Y2 - 24 April 2013 through 28 April 2013

ER -

Direct production of nanostructured copper-nickel (Cu-Ni) alloy particles

Abstract

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Keywords

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