Determination of boron in Turkish wines by microwave plasma atomic emission spectrometry

Nil Ozbek; Suleyman Akman

doi:10.1016/j.lwt.2014.11.047

Determination of boron in Turkish wines by microwave plasma atomic emission spectrometry

Nil Ozbek, Suleyman Akman^*

^*Corresponding author for this work

Department of Chemical Engineering

Istanbul Technical University

Research output: Contribution to journal › Article › peer-review

34 Citations (Scopus)

Abstract

Boron in various Turkish red wine and white wine samples was determined by microwave plasma-atomic emission spectrometry (MP-AES) at 249.677nm. MP-AES is a novel instrument which provides a low-cost analysis based on a micro-wave plasma generated with nitrogen. Wine samples were not pre-treated prior to analysis. The recovery rate of boron added to the 1:1 diluted wine samples was around 80% which showed interference due to the matrix of the wine samples. Therefore standard addition method was used for quantifications. The limit of detection and limit of quantification were 0.08 and 0.28μgmL^-1, respectively. A satisfactory linearity (r²>0.999) was obtained up to 10mgL^-1 of boron. The range of boron concentrations in various wine samples was 4.2-10.8mgL^-1.

Original language	English
Pages (from-to)	532-535
Number of pages	4
Journal	LWT
Volume	61
Issue number	2
DOIs	https://doi.org/10.1016/j.lwt.2014.11.047
Publication status	Published - 1 May 2015

Bibliographical note

Publisher Copyright:
© 2014 Elsevier Ltd.

Keywords

Boron
Microwave plasma -atomic emission spectrometry
Wine

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10.1016/j.lwt.2014.11.047

Cite this

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abstract = "Boron in various Turkish red wine and white wine samples was determined by microwave plasma-atomic emission spectrometry (MP-AES) at 249.677nm. MP-AES is a novel instrument which provides a low-cost analysis based on a micro-wave plasma generated with nitrogen. Wine samples were not pre-treated prior to analysis. The recovery rate of boron added to the 1:1 diluted wine samples was around 80% which showed interference due to the matrix of the wine samples. Therefore standard addition method was used for quantifications. The limit of detection and limit of quantification were 0.08 and 0.28μgmL-1, respectively. A satisfactory linearity (r2>0.999) was obtained up to 10mgL-1 of boron. The range of boron concentrations in various wine samples was 4.2-10.8mgL-1.",

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AU - Ozbek, Nil

AU - Akman, Suleyman

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AB - Boron in various Turkish red wine and white wine samples was determined by microwave plasma-atomic emission spectrometry (MP-AES) at 249.677nm. MP-AES is a novel instrument which provides a low-cost analysis based on a micro-wave plasma generated with nitrogen. Wine samples were not pre-treated prior to analysis. The recovery rate of boron added to the 1:1 diluted wine samples was around 80% which showed interference due to the matrix of the wine samples. Therefore standard addition method was used for quantifications. The limit of detection and limit of quantification were 0.08 and 0.28μgmL-1, respectively. A satisfactory linearity (r2>0.999) was obtained up to 10mgL-1 of boron. The range of boron concentrations in various wine samples was 4.2-10.8mgL-1.

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Determination of boron in Turkish wines by microwave plasma atomic emission spectrometry

Abstract

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Keywords

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