TY - JOUR
T1 - Characterization investigations of melt-spun ternary Al-xSi-3.3Fe (x=10, 20 wt.%) alloys
AU - Ünlü, N.
AU - Genç, A.
AU - Öveçoǧlu, M. L.
AU - Eruslu, N.
AU - Froes, F. H.
PY - 2001/6/28
Y1 - 2001/6/28
N2 - Two ternary Al-xSi-3.3Fe alloys, one with the hypoeutectic (x=10 wt.% Si) and the other with the hypereutectic (x=20 wt.% Si) composition were rapidly quenched from the melt at cooling rates between 106 and 107 K/s using the melt-spinning technique. The resulting melt-spun ribbons were characterized using optical microscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD) and microhardness techniques. On the basis of the Al peak shifts measured in the XRD scans, solid solubility extension values of 3.01 and 2.97 at.% Si in Al were determined for the hypoeutectic and hypereutectic alloy, respectively. Whereas SEM investigations showed the presence of dendrites rich in Al, TEM investigations revealed nanosized spherically-shaped Si crystals 5-10 nm in size in the hypoeutectic alloy and those equiaxed in shape having a size range between 50 and 70 nm. Both XRD and TEM investigations confirmed the absence of any intermetallic phase formation for both alloys. The microhardness values of the hypoeutectic and hypereutectic ternary Al-Si-Fe alloys were measured as 251 and 297 kg/mm2, respectively.
AB - Two ternary Al-xSi-3.3Fe alloys, one with the hypoeutectic (x=10 wt.% Si) and the other with the hypereutectic (x=20 wt.% Si) composition were rapidly quenched from the melt at cooling rates between 106 and 107 K/s using the melt-spinning technique. The resulting melt-spun ribbons were characterized using optical microscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD) and microhardness techniques. On the basis of the Al peak shifts measured in the XRD scans, solid solubility extension values of 3.01 and 2.97 at.% Si in Al were determined for the hypoeutectic and hypereutectic alloy, respectively. Whereas SEM investigations showed the presence of dendrites rich in Al, TEM investigations revealed nanosized spherically-shaped Si crystals 5-10 nm in size in the hypoeutectic alloy and those equiaxed in shape having a size range between 50 and 70 nm. Both XRD and TEM investigations confirmed the absence of any intermetallic phase formation for both alloys. The microhardness values of the hypoeutectic and hypereutectic ternary Al-Si-Fe alloys were measured as 251 and 297 kg/mm2, respectively.
KW - Hypo- and hypereutectic Al-Si-Fe alloys
KW - Melt-spinning
KW - Ternary Al-Si-Fe system
UR - http://www.scopus.com/inward/record.url?scp=0035963595&partnerID=8YFLogxK
U2 - 10.1016/S0925-8388(01)01196-3
DO - 10.1016/S0925-8388(01)01196-3
M3 - Article
AN - SCOPUS:0035963595
SN - 0925-8388
VL - 322
SP - 249
EP - 256
JO - Journal of Alloys and Compounds
JF - Journal of Alloys and Compounds
IS - 1-2
ER -