Amonyum floroborat üretimi ve üretim parametrelerinin belirlenmesi

Translated title of the contribution: Ammonium fluoroborate production and determination of production parameters

A. Abdullah Ceyhan*, Safiye Bağcı, Orhan Baytar, Ömer Şahin

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

4 Citations (Scopus)

Abstract

In this study, the production parameters of ammonium fluoroborate (NH4BF4) synthesis with reaction between boric acid and ammonium hydrogen fluoride were investigated. For this purpose, the effects of parameters such as reactive feeding ratio, reaction temperature, stirring rate, stirrer type, second solvent effect determined separately. Surface morphologies and structural analysis of the crystals obtained after reaction were determined by XRD, FT-IR and SEM analysis respectively. The optimum production conditions were found as reactant feeding rate 1:2, reaction temperature 90 °C, stirring type hot air stirring. Limited oxygen index test results showed that ammonium fluoroborate exhibits excellent flame retardance.

Translated title of the contributionAmmonium fluoroborate production and determination of production parameters
Original languageTurkish
Pages (from-to)63-72
Number of pages10
JournalJournal of Boron
Volume5
Issue number2
DOIs
Publication statusPublished - 29 Jun 2020
Externally publishedYes

Bibliographical note

Publisher Copyright:
© 2020, Turkish Energy Nuclear and Mining Research Institute. All rights reserved.

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