A Practical Method for the Determination of Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in Different Types of Vinegars by Microwave Induced Plasma Optical Emission Spectrometry

Nil Ozbek; Merve Koca; Suleyman Akman

doi:10.1007/s12161-016-0421-x

A Practical Method for the Determination of Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in Different Types of Vinegars by Microwave Induced Plasma Optical Emission Spectrometry

Nil Ozbek^*, Merve Koca, Suleyman Akman

^*Corresponding author for this work

Department of Chemical Engineering

Istanbul Technical University

Research output: Contribution to journal › Article › peer-review

19 Citations (Scopus)

Abstract

A practical method was described for determining Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in various vinegar samples using microwave induced plasma optical emission spectrometry (MIP OES). Prior to analysis, vinegar samples were diluted to appropriate volumes and then directly aspirated to the plasma. All determinations were performed using aqueous standards for calibration. The analytes added to the vinegar samples were recovered quantitatively (between 93 and 104 %). The LOD values for Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn were 0.62, 7.67, 4.55, 0.52, 1.22, 5.72, 1.32, 0.35, 2.42, and 26.0 μg L⁻¹, respectively. Finally, the analyte concentrations in various types of vinegar samples produced in Turkey were determined and found below maximum allowable values stated by the Turkish Food Codex.

Original language	English
Pages (from-to)	2246-2250
Number of pages	5
Journal	Food Analytical Methods
Volume	9
Issue number	8
DOIs	https://doi.org/10.1007/s12161-016-0421-x
Publication status	Published - 1 Aug 2016

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Publisher Copyright:
© 2016, Springer Science+Business Media New York.

Keywords

Al
B
Co
Cr
Cu
Fe
Mg
Microwave-induced plasma optical emission spectrometry
Mn
Pb
Vinegar
Zn

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10.1007/s12161-016-0421-x

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title = "A Practical Method for the Determination of Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in Different Types of Vinegars by Microwave Induced Plasma Optical Emission Spectrometry",

abstract = "A practical method was described for determining Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in various vinegar samples using microwave induced plasma optical emission spectrometry (MIP OES). Prior to analysis, vinegar samples were diluted to appropriate volumes and then directly aspirated to the plasma. All determinations were performed using aqueous standards for calibration. The analytes added to the vinegar samples were recovered quantitatively (between 93 and 104 %). The LOD values for Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn were 0.62, 7.67, 4.55, 0.52, 1.22, 5.72, 1.32, 0.35, 2.42, and 26.0 μg L−1, respectively. Finally, the analyte concentrations in various types of vinegar samples produced in Turkey were determined and found below maximum allowable values stated by the Turkish Food Codex.",

keywords = "Al, B, Co, Cr, Cu, Fe, Mg, Microwave-induced plasma optical emission spectrometry, Mn, Pb, Vinegar, Zn",

author = "Nil Ozbek and Merve Koca and Suleyman Akman",

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doi = "10.1007/s12161-016-0421-x",

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T1 - A Practical Method for the Determination of Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in Different Types of Vinegars by Microwave Induced Plasma Optical Emission Spectrometry

AU - Ozbek, Nil

AU - Koca, Merve

AU - Akman, Suleyman

PY - 2016/8/1

Y1 - 2016/8/1

N2 - A practical method was described for determining Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in various vinegar samples using microwave induced plasma optical emission spectrometry (MIP OES). Prior to analysis, vinegar samples were diluted to appropriate volumes and then directly aspirated to the plasma. All determinations were performed using aqueous standards for calibration. The analytes added to the vinegar samples were recovered quantitatively (between 93 and 104 %). The LOD values for Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn were 0.62, 7.67, 4.55, 0.52, 1.22, 5.72, 1.32, 0.35, 2.42, and 26.0 μg L−1, respectively. Finally, the analyte concentrations in various types of vinegar samples produced in Turkey were determined and found below maximum allowable values stated by the Turkish Food Codex.

AB - A practical method was described for determining Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in various vinegar samples using microwave induced plasma optical emission spectrometry (MIP OES). Prior to analysis, vinegar samples were diluted to appropriate volumes and then directly aspirated to the plasma. All determinations were performed using aqueous standards for calibration. The analytes added to the vinegar samples were recovered quantitatively (between 93 and 104 %). The LOD values for Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn were 0.62, 7.67, 4.55, 0.52, 1.22, 5.72, 1.32, 0.35, 2.42, and 26.0 μg L−1, respectively. Finally, the analyte concentrations in various types of vinegar samples produced in Turkey were determined and found below maximum allowable values stated by the Turkish Food Codex.

KW - Al

KW - B

KW - Co

KW - Cr

KW - Cu

KW - Fe

KW - Mg

KW - Microwave-induced plasma optical emission spectrometry

KW - Mn

KW - Pb

KW - Vinegar

KW - Zn

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DO - 10.1007/s12161-016-0421-x

M3 - Article

AN - SCOPUS:84955290036

SN - 1936-9751

VL - 9

SP - 2246

EP - 2250

JO - Food Analytical Methods

JF - Food Analytical Methods

IS - 8

ER -

A Practical Method for the Determination of Al, B, Co, Cr, Cu, Fe, Mg, Mn, Pb, and Zn in Different Types of Vinegars by Microwave Induced Plasma Optical Emission Spectrometry

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Keywords

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