A new approach for the determination of sulphur in airborne particles by HR-CS ETAAS

Nil Ozbek; Asli Baysal

doi:10.1080/03067319.2016.1180381

A new approach for the determination of sulphur in airborne particles by HR-CS ETAAS

Nil Ozbek
, Asli Baysal^*

^*Corresponding author for this work

Department of Chemical Engineering

Istanbul Aydin University

Research output: Contribution to journal › Article › peer-review

10 Citations (Scopus)

Abstract

In this work, water and nitric acid extractable sulphur concentrations in PM2.5 fraction of urban aerosols were determined by high-resolution continuum source electrothermal molecular absorption spectrometry using most suitable CS molecular absorption band at 258.056 nm. For this purpose, the PM2.5 airborne particulates were collected on quartz filters using a high-volume sampler (500 L/min) in Istanbul (Turkey) during six months (January–June) of two consecutive years. The instrumental and experimental parameters (pyrolysis temperature, molecule formation temperature and leaching reagents) were optimised. The validity of the method for the sulphur was tested using standard reference material and the results were found to be in the uncertainty limits of the certified value.

Original language	English
Pages (from-to)	505-514
Number of pages	10
Journal	International Journal of Environmental Analytical Chemistry
Volume	96
Issue number	6
DOIs	https://doi.org/10.1080/03067319.2016.1180381
Publication status	Published - 2 May 2016

Bibliographical note

Publisher Copyright:
© 2016 Informa UK Limited, trading as Taylor & Francis Group.

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 11 Sustainable Cities and Communities

Keywords

Airborne particulate matter
High-resolution continuum source electrothermal atomic absorption spectrometry
Pm2.5
Sulphur

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10.1080/03067319.2016.1180381

Cite this

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title = "A new approach for the determination of sulphur in airborne particles by HR-CS ETAAS",

abstract = "In this work, water and nitric acid extractable sulphur concentrations in PM2.5 fraction of urban aerosols were determined by high-resolution continuum source electrothermal molecular absorption spectrometry using most suitable CS molecular absorption band at 258.056 nm. For this purpose, the PM2.5 airborne particulates were collected on quartz filters using a high-volume sampler (500 L/min) in Istanbul (Turkey) during six months (January{\textendash}June) of two consecutive years. The instrumental and experimental parameters (pyrolysis temperature, molecule formation temperature and leaching reagents) were optimised. The validity of the method for the sulphur was tested using standard reference material and the results were found to be in the uncertainty limits of the certified value.",

keywords = "Airborne particulate matter, High-resolution continuum source electrothermal atomic absorption spectrometry, Pm2.5, Sulphur",

author = "Nil Ozbek and Asli Baysal",

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AU - Baysal, Asli

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N2 - In this work, water and nitric acid extractable sulphur concentrations in PM2.5 fraction of urban aerosols were determined by high-resolution continuum source electrothermal molecular absorption spectrometry using most suitable CS molecular absorption band at 258.056 nm. For this purpose, the PM2.5 airborne particulates were collected on quartz filters using a high-volume sampler (500 L/min) in Istanbul (Turkey) during six months (January–June) of two consecutive years. The instrumental and experimental parameters (pyrolysis temperature, molecule formation temperature and leaching reagents) were optimised. The validity of the method for the sulphur was tested using standard reference material and the results were found to be in the uncertainty limits of the certified value.

AB - In this work, water and nitric acid extractable sulphur concentrations in PM2.5 fraction of urban aerosols were determined by high-resolution continuum source electrothermal molecular absorption spectrometry using most suitable CS molecular absorption band at 258.056 nm. For this purpose, the PM2.5 airborne particulates were collected on quartz filters using a high-volume sampler (500 L/min) in Istanbul (Turkey) during six months (January–June) of two consecutive years. The instrumental and experimental parameters (pyrolysis temperature, molecule formation temperature and leaching reagents) were optimised. The validity of the method for the sulphur was tested using standard reference material and the results were found to be in the uncertainty limits of the certified value.

KW - Airborne particulate matter

KW - High-resolution continuum source electrothermal atomic absorption spectrometry

KW - Pm2.5

KW - Sulphur

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M3 - Article

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SN - 0306-7319

VL - 96

SP - 505

EP - 514

JO - International Journal of Environmental Analytical Chemistry

JF - International Journal of Environmental Analytical Chemistry

IS - 6

ER -

A new approach for the determination of sulphur in airborne particles by HR-CS ETAAS

Abstract

Bibliographical note

UN SDGs

Keywords

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